HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichloroethane → HCID 118511020, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichloroethane | HCID 11 | — |
| Reactant | 2-Naphthoyl chloride | HCID 75246 | — |
| Reactant | 1-Methoxypyrene | HCID 160236 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 118511020 | HCID 118511020 | — |
Reaction Steps
Methoxy pyrene (23.20 g, 0.1 mol), 2-naphthoyl chloride (56.8 g, 0.333 mol), and 1,2-dichloroethane (325 g) were put in a flask. Then, aluminum chloride (29.4 g, 0.12 mol) was slowly added to the solution at ambient temperature, and the mixture was agitated for 2 hours. When the reaction was terminated, a precipitate obtained by adding methanol thereto was filtered, obtaining 2-naphthoyl methoxy pyrene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09371444B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-91f01e50c4e5470eb1753a1659ee35c0 |
| Source note | uspto-grants-2016_06 |