HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66678332, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 59536826 | HCID 59536826 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 66678332 | HCID 66678332 | — |
Reaction Steps
Of the compound from Example 79A, 150 mg (0.47 mmol) were stirred for 20 min in 3 ml of a 4N solution of hydrogen chloride in dioxane. The volatile components were removed on a rotary evaporator and the residue was dried in an HV. This gave 140 mg (87% purity) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08202895B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-95051fc9e06e4a8b997d6aaf8448f5a1 |
| Source note | uspto-grants-2012_06 |