HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfone → tert-Butyl {2-(methylsulphonyl)-1-[3-(trifluoromethyl)phenyl]ethyl}carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfone | HCID 6213 | — |
| Reactant | tert-butyl (NE)-N-[[3-(trifluoromethyl)phenyl]methylidene]carbamate | HCID 46855703 | — |
| Product | tert-Butyl {2-(methylsulphonyl)-1-[3-(trifluoromethyl)phenyl]ethyl}carbamate | HCID 59536720 | — |
Reaction Steps
From 1.50 g (15.9 mmol) of (methylsulphonyl)methane and 1.45 g (5.31 mmol) of the compound from Example 11A, using the same process as for Example 117A, 535 mg (27% of theory) of the title compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08202895B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-f03fbe80d2d24fa1aa6419acf96d2586 |
| Source note | uspto-grants-2012_06 |