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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2206633Generated: November 1, 2026

HCID 10703244, compound → HCID 12915443, compound

https://huagongshe.com/reaction/2206633

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 10703244HCID 10703244—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 12915443HCID 1291544399%

Reaction Steps

Methyl 2-vinyl-1H-indole-3-carboxylate (80 mg, 0.4 mmol) and 10% palladium on charcoal (100 mg) in methanol (30 mL) were stirred under hydrogen 0.2 MPa at room temperature for 15 hours. The mixture was filterated the solid and concentrated in vacuum to obtain methyl 2-ethyl-1H-indole-3-carboxylate as a white solid (79 mg, 99%) LRMS (M+H+) m/z: calcd 203.1 found 203.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09371331B2
Source datasetuspto-grants-2016_06
ORD IDord-203afddc55f74a9c9c0a0bcc1443ef45
Source noteuspto-grants-2016_06