HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrazinemethanol → Pyrazin-2-ylmethyl methanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrazinemethanol | HCID 201734 | — |
| Reactant | Methanesulfonic acid pyrimidin-5-ylmethyl ester | HCID 86610239 | — |
| Product | Pyrazin-2-ylmethyl methanesulfonate | HCID 15096999 | — |
Reaction Steps
Pyrazin-2-ylmethyl methanesulfonate was prepared in a similar manner as used to prepare pyrimidin-5-ylmethyl methanesulfonate using pyrazin-2-ylmethanol instead of pyrimidin-5-ylmethanol. LCMS-ESI+ (m/z): [M+H]+ calc'd for C6H8N2O3S: 189.03; found: 189.01.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09376392B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-c002239bd8a647cbb22c35e234e26b1b |
| Source note | uspto-grants-2016_06 |