HRID2207106

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID9773

Ethanamine, 2,2,2-trifluoro-

C2H4F3N

HCID79177

Acetic acid, bromo-, 1,1-dimethylethyl ester

C6H11BrO2

PRODUCTS

生成物

HCID60680127

未命名化合物

收率 74%

PROCEDURE

实验过程

The subtitled compound was synthesized by the method of example 15 step (i) from tert-butyl bromoacetate (13.6 g) and 2,2,2-trifluoroethylamine (8.9 g). The sub-title compound (11 g) was obtained as a colourless oil; 1H NMR (300 MHz, CDCl3); 3.39 (2H, s), 3.20 (2H, q, J=9.4 Hz), 1.44 (9H, s).