HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → 4-(Benzylamino)but-3-en-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 3-Buten-2-one, 4-methoxy- | HCID 94297 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 4-(Benzylamino)but-3-en-2-one | HCID 521443 | 70% |
Reaction Steps
A mixture of benzylamine (1.1 mL, 10 mmol) and 4-methoxybut-3-en-2-one (1 mL, 10 mmol) in chloroform (100 mL) was stirred at room temperature until complete conversion. Then, the solvent was evaporated to afford the desired product 30 in 70% yield which was used without additional purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09376387B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-6983509c973240aca8c91fe06bd0f612 |
| Source note | uspto-grants-2016_06 |