HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzylamine → HCID 131735879, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzylamine | HCID 66648 | — |
| Reactant | 3-Buten-2-one, 4-methoxy- | HCID 94297 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131735879 | HCID 131735879 | 100% |
Reaction Steps
A solution of 4-methoxy-3-buten-2-one (100.1 mg, 1 mmol) and 2-chlorobenzylamine (141.6 mg, 1 mmol) in dry CH2Cl2 (5 mL) is stirred under reflux for 2 h. The solvent is evaporated under reduced pressure to afford the title compound 45 as a yellow oil (Yield 209 mg, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09376387B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-3a4a2ce75550446d87ae63d6a7fffe13 |
| Source note | uspto-grants-2016_06 |