HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenemethanamine, 3-chloro- → 4-[(3-Chlorophenyl)methylamino]but-3-en-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenemethanamine, 3-chloro- | HCID 77802 | — |
| Reactant | 3-Buten-2-one, 4-methoxy- | HCID 94297 | — |
| Product | 4-[(3-Chlorophenyl)methylamino]but-3-en-2-one | HCID 131735882 | — |
Reaction Steps
The title compound 64 is prepared according to the procedure reported in step A of Example 18 with 4-methoxy-3-buten-2-one (0.1 g, 1 mmol) and 3-chlorobenzylamine (0.138 g, 1 mmol) as reactants. Yellow oil. (Yield 0.21 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09376387B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-92e4cc37b1c94880b485f31b6e8d8d9a |
| Source note | uspto-grants-2016_06 |