HuagongsheHuagongshe Chemistry Print Report · For research reference only
Crotonaldehyde → HCID 90304014, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Crotonaldehyde | HCID 447466 | — |
| Reactant | HCID 90303965 | HCID 90303965 | — |
| Product | HCID 90304014 | HCID 90304014 | — |
Reaction Steps
The title compound 76 is prepared according to the procedure reported in step C of Example 8 with tetralone 75 (130 mg, 0.56 mmol) and crotonaldehyde (0.19 mL, 2.24 mmol) as reactants. Purification by column chromatography on SiO2 (Petroleum/diethyl ether=1:1) afford the title compound 76 as an off-white solid. (Yield 121 mg, 83%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09376387B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-ece5c96b6fd24e7181d2dc35ca566e3f |
| Source note | uspto-grants-2016_06 |