HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 11195631, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | 5,6-Dimethoxy-1-indanone | HCID 75018 | — |
| Product | HCID 11195631 | HCID 11195631 | — |
Reaction Steps
The title compound 78 is prepared according to the procedure reported in step A of Example 17 with 5,6-dimethoxy-1-indanone (1 g, 5.2 mmol) and allyl bromide (0.86 mL, 7.17 mmol) as reactants. Purification by column chromatography on SiO2 (Petroleum Ether/EtOAc=2:1) afford the title compound 78 as a colorless oil. (Yield 0.5 g, 46%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09376387B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-8b2a29bd008f469eacb2f7990b538d9b |
| Source note | uspto-grants-2016_06 |