HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2E)-2-[(3-bromo-4-pyridyl)methylene]-6,7-dimethoxy-tetralin-1-one → 2-[(3-Bromo-4-pyridyl)methyl]-6,7-dimethoxy-tetralin-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2E)-2-[(3-bromo-4-pyridyl)methylene]-6,7-dimethoxy-tetralin-1-one | HCID 118557935 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Product | 2-[(3-Bromo-4-pyridyl)methyl]-6,7-dimethoxy-tetralin-1-one | HCID 118557859 | — |
Reaction Steps
The title compound 100 is prepared according to the procedure reported in Example 36.1 with compound 84 (374 mg, 1.0 mmol) and Pt/C (5 wt % loading, 38 mg) as reactants. White solid. (Yield 0.251 g, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09376387B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-e3218ee2c9184bf2900f8cb7a9edd54e |
| Source note | uspto-grants-2016_06 |