HCID 118558005, compound → HCID 118557804, compound

HRID 2207196Notes

Reaction equation

HRID 2207196 reaction equation
[Cl:1][C:2]1[CH:3]=[N:4][CH:5]=[CH:6][C:7]=1/[CH:8]=[C:9]1/[C:10](=[O:23])[C:11]2[C:16]([CH2:17][CH2:18]/1)=[CH:15][C:14]([O:19][CH3:20])=[C:13]([O:21][CH3:22])[CH:12]=2>[Pt]>[Cl:1][C:2]1[CH:3]=[N:4][CH:5]=[CH:6][C:7]=1[CH2:8][CH:9]1[CH2:18][CH2:17][C:16]2[C:11](=[CH:12][C:13]([O:21][CH3:22])=[C:14]([O:19][CH3:20])[CH:15]=2)[C:10]1=[O:23]

Participants

3

Reactant 1

HCID 118558005HCID 118558005, compound

Product 1

HCID 118557804HCID 118557804, compound

Reagents, catalysts & solvents 1

HCID 23939PlatinumCatalyst

Procedure

The title compound 101 is prepared according to the procedure reported in Example 36.1 with compound 85 (93 mg, 2.83 mmol) and Pt/C (5 wt/o loading, 93 mg) as reactants. White solid. (Yield 0.47 g, 51%).

Sources & evidence

ORD record
ord-2eec3c9ff4004c678fa617bc472351fc
Source dataset
uspto-grants-2016_06
Patent number
US09376387B2

Reaction notes

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