HCID 118558028, compound → HCID 118557926, compound

HRID 2207201Notes

Reaction equation

HRID 2207201 reaction equation
[Br:1][C:2]1[CH:3]=[N:4][CH:5]=[CH:6][C:7]=1/[CH:8]=[C:9]1/[C:10](=[O:20])[C:11]2[C:16]([CH2:17]/1)=[CH:15][C:14]([CH3:18])=[C:13]([CH3:19])[CH:12]=2>[Pt]>[Br:1][C:2]1[CH:3]=[N:4][CH:5]=[CH:6][C:7]=1[CH2:8][CH:9]1[CH2:17][C:16]2[C:11](=[CH:12][C:13]([CH3:19])=[C:14]([CH3:18])[CH:15]=2)[C:10]1=[O:20]

Participants

3

Reactant 1

HCID 118558028HCID 118558028, compound

Product 1

HCID 118557926HCID 118557926, compound

Reagents, catalysts & solvents 1

HCID 23939PlatinumCatalyst

Procedure

The title compound 107 is prepared according to the procedure reported in Example 37.2 with compound 92 (0.44 g, 1.35 mmol) and Pt/C (5 wt % loading, 44 mg) as reactants. White solid. (Yield 0.39 g, 89%).

Sources & evidence

ORD record
ord-7fe6faa741ac453aa7c9bd14592dae6a
Source dataset
uspto-grants-2016_06
Patent number
US09376387B2

Reaction notes

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