HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → 2-[(3-Actyl-1-benzyl-pyridin-1-ium-4-yl)methyl]-6,7-dimethoxy-tetralin-1-one bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | 2-[(3-Acetyl-4-pyridyl)methyl]-6,7-dimethoxy-tetralin-1-one | HCID 118558021 | — |
| Product | 2-[(3-Actyl-1-benzyl-pyridin-1-ium-4-yl)methyl]-6,7-dimethoxy-tetralin-1-one bromide | HCID 131735884 | — |
Reaction Steps
The title compound 132 is prepared according to the procedure reported in Example 38.1 with compound 104 (93 mg, 0.27 mmol) and benzyl bromide (66 μL, 0.54 mmol) as reactants. White solid. (Yield 117.1 mg, 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09376387B2 |
| Source dataset | uspto-grants-2016_06 |
| ORD ID | ord-f1995642446840129bb9f137cc4819fe |
| Source note | uspto-grants-2016_06 |