HCID 89649674, compound → HCID 89649543, compound

Participants

Reaction Steps

A solution of 1-benzyloxy-5-ethoxy-2,3-difluoro-benzene (which may be prepared as described in Description 60) (546 mg, 2.07 mmol) in methanol (10 mL) was passed through a 10% Pd—C H-cube cartridge at 1 ml/min. The solution was passed through the H-cube a second time. Chromatography on silica (elution with DCM) gave 5-ethoxy-2,3-difluoro-phenol (D61) (270 mg);

Provenance & Evidence