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HRID2207858

反应详情

EQUATION

反应方程式

HRID 2207858 的结构方程式

REACTANTS

反应物

3
结构：CC(=O)O
HCID176

Acetic Acid

C2H4O2

结构：O=C([O-])[O-].[Na+].[Na+]
HCID10340

Carbonic acid sodium salt (1:2)

CNa2O3

2 次

结构：NC(=O)C1=CN([C@@H]2O[C@H](COP(=O)(O)OP(=O)(O)OC[C@H]3O[C@@H](n4cnc5c(N)ncnc54)[C@H](O)[C@@H]3O)[C@@H](O)[C@H]2O)C=CC1
HCID439153

Adenosine 5'-(trihydrogen diphosphate), P'→5'-ester with 1,4-dihydro-1-.beta.-D-ribofuranosyl-3-pyridinecarboxamide

C21H29N7O14P2

PRODUCTS

生成物

1
结构：CC(=O)O[C@H]1C(O)O[C@H](COP(=O)(O)OP(=O)(O)OC[C@H]2O[C@@H](n3cnc4c(N)ncnc43)[C@H](O)[C@@H]2O)[C@H]1O
HCID72193709

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

CONDITIONS

反应条件

温度
85 °C

PROCEDURE

实验过程

To 80 mg of Na2CO3 was added 2 mL of glacial acetic acid. The mixture was stirred at 85° C. until all the Na2CO3 reacted. 250 mg of NAD was added and the mixture was stirred at 85° C. for 15 min, cooled to below 75° C. and diluted with 20 mL of CH3CN. The precipitate was filtered, suspended in 5 mL of CH3CN, and filtered again to give crude OAADPR.

WORKUP

后处理

  1. customreacted
  2. temperaturecooled to below 75° C.
  3. filtrationThe precipitate was filtered
  4. filtrationfiltered again