Bromomethylcyclopropane → HCID 67956353, compound

HRID 2208134Notes

Reaction equation

[Br:1][C:2]1[CH:7]=[C:6]([CH3:8])[C:5]([F:9])=[CH:4][C:3]=1[OH:10].Br[CH2:12][CH:13]1[CH2:15][CH2:14]1>>[Br:1][C:2]1[CH:7]=[C:6]([CH3:8])[C:5]([F:9])=[CH:4][C:3]=1[O:10][CH2:12][CH:13]1[CH2:15][CH2:14]1

Participants

Reactant 2

HCID 81503Bromomethylcyclopropane

HCID 67032927HCID 67032927, compound

Product 1

HCID 67956353HCID 67956353, compound

Procedure

Starting from 2-bromo-5-fluoro-4-methyl-phenol (example B.a3) and commercially available bromomethyl-cyclopropane the title compound is obtained as colorless oil after distillation at 5×10−3 mbar.

Sources & evidence

ORD record: ord-3705f8de7dcf4fd8b63354a265e07380
Source dataset: uspto-grants-2016_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09376442B2

Reaction notes

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