Bromomethylcyclopropane → HCID 67033133, compound

HRID 2208139Notes

Reaction equation

HRID 2208139 reaction equation
[Br:1][C:2]1[CH:7]=[C:6]([CH:8]([CH3:10])[CH3:9])[CH:5]=[CH:4][C:3]=1[OH:11].Br[CH2:13][CH:14]1[CH2:16][CH2:15]1>>[Br:1][C:2]1[CH:7]=[C:6]([CH:8]([CH3:9])[CH3:10])[CH:5]=[CH:4][C:3]=1[O:11][CH2:13][CH:14]1[CH2:16][CH2:15]1

Participants

3

Reactant 2

HCID 81503BromomethylcyclopropaneHCID 149691732-Bromo-4-(propan-2-yl)phenol

Product 1

HCID 67033133HCID 67033133, compound

Procedure

Starting from 2-bromo-4-isopropyl-phenol (example B.a6) and commercially available bromomethyl-cyclopropane the title compound is obtained as colorless solid after short path distillation at 2×10−3 mbar.

Sources & evidence

ORD record
ord-5cbb7004c33d41c59101dc18470f95d7
Source dataset
uspto-grants-2016_06
Patent number
US09376442B2

Reaction notes

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