HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 22089Generated: October 27, 2026
4-Coumaric acid → 2-Propenoic acid, 3-phenyl-
https://huagongshe.com/reaction/22089
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Coumaric acid | HCID 322 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Glycidol | HCID 11164 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Solvent | Glycerol | HCID 753 | — |
| Product | 2-Propenoic acid, 3-phenyl- | HCID 8784 | — |
Reaction Steps
17.4 g of p-hydroxy cinnamic acid and 40.0 g of glycidol were dissolved in 20 ml of DMSO, and catalytic amount of sulfuric acid was added. The solution was heated to 90° C. and then heating and agitation was carried out for 3 hours, neutralized by adding sodium hydroxide and then adduct of cinnamic acid and glycerin was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05426210 |
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| Source dataset | uspto-grants-1995_06 |
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| ORD ID | ord-9fd1cb87e984445880ac895829b5f575 |
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| Source note | uspto-grants-1995_06 |
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