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HRID2209109

反应详情

EQUATION

反应方程式

HRID 2209109 的结构方程式

REACTANTS

反应物

2
结构：C1NCC2CC1O2
HCID17965857

6-Oxa-3-azabicyclo[3.1.1]heptane

C5H9NO

结构：CC(C)(C)OC(=O)N1C2CC1CN(c1ccc(Br)cc1)C2
HCID117843577

未命名化合物

PRODUCTS

生成物

1
结构：Brc1ccc(N2CC3CC(C2)O3)cc1
HCID84804635

未命名化合物

收率 61%

PROCEDURE

实验过程

Prepared by the procedure, previously described for the synthesis of tert-butyl 3-(4-bromophenyl)-3,6-diazabicyclo[3.1.1]heptane-6-carboxylate, using instead 6-oxa-3-azabicyclo[3.1.1]heptane as a starting material to afford 570.0 mg (61%) of 3-(4-bromophenyl)-6-oxa-3-azabicyclo[3.1.1]heptane.

WORKUP

后处理

  1. customPrepared by the procedure