HRID2209142

反应详情

EQUATION

反应方程式

HRID 2209142 的结构方程式

CONDITIONS

反应条件

温度
100 °C

PROCEDURE

实验过程

To a round-bottomed flask equipped with a stifling bar and a N2 tee, 3-iodo-1H-pyrazole (2.00 g, 10 mmol), 2-methylpropan-2-ol (7.64 g, 103 mmol), and concentrated sulfuric acid (1.08 g, 11 mmol) were added. The resulting mixture was heated at 100° C. for 3 hrs.

WORKUP

后处理

  1. customTo a round-bottomed flask equipped with a stifling bar