HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 3,6-bis(2-Chlorophenyl)-1,2-dihydro-1-methyl-1,2,4,5-tetrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Bis(alpha,2-dichlorobenzylidene)hydrazine | HCID 150853 | — |
| Reactant | Methylhydrazine sulfate | HCID 165286 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3,6-bis(2-Chlorophenyl)-1,2-dihydro-1-methyl-1,2,4,5-tetrazine | HCID 12912716 | — |
Reaction Steps
The suspension containing 3.74 g (0.026 mol) of methylhydrazine sulfate, 11.9 ml (0.086 mol) of triethylamine in 11.2 ml of abs. ethanol is boiled under reflux while portionwise adding 1.12 g (0.0032 mol) of bis(alpha,2-dichlorobenzylidene)hydrazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05455237 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-dc737d946fda42009b06b406289dfb1e |
| Source note | uspto-grants-1995_10 |