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HRID2209423

反应详情

EQUATION

反应方程式

HRID 2209423 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：ClC(=NN=C(Cl)c1ccccc1Cl)c1ccccc1Cl
HCID150853

未命名化合物

结构：CNN.O=S(=O)(O)O
HCID165286

Methylhydrazine sulfate

CH8N2O4S

PRODUCTS

生成物

1
结构：CN1NC(c2ccccc2Cl)=NN=C1c1ccccc1Cl
HCID12912716

3,6-Bis(2-chlorophenyl)-1,2-dihydro-1-methyl-1,2,4,5-tetrazine

C15H12Cl2N4

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

The suspension containing 3.74 g (0.026 mol) of methylhydrazine sulfate, 11.9 ml (0.086 mol) of triethylamine in 11.2 ml of abs. ethanol is boiled under reflux while portionwise adding 1.12 g (0.0032 mol) of bis(alpha,2-dichlorobenzylidene)hydrazine.

WORKUP

后处理

  1. temperatureunder reflux