HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitrogen → 2-Propenoic acid, 3-phenyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitrogen | HCID 947 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Trimethoxy cinnamic acid | HCID 54572276 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 2-Propenoic acid, 3-phenyl- | HCID 8784 | — |
Reaction Steps
4.35 g of trimethoxy cinnamic acid and 100 mg of sodium hydroxide were dissolved in 5 ml of DMSO, and the mixture was stirred and heated to 90° C. under a flow of N2 gas. Water in the system was removed under low pressure condition. 10 g of glycidol was added, heating and agitation was carried out for 3 hours, and then the adduct of cinnamic acid and glycerin was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05426210 |
| Source dataset | uspto-grants-1995_06 |
| ORD ID | ord-6d8fcbd9ccb7401eb76af8001a00d099 |
| Source note | uspto-grants-1995_06 |