HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 1-(9,10-Dihydro-9,10-methanoanthracen-9-ylmethyl)piperidin-4-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 21480612 | HCID 21480612 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 1-(9,10-Dihydro-9,10-methanoanthracen-9-ylmethyl)piperidin-4-ol | HCID 21480617 | 88% |
Reaction Steps
Using a procedure similar to that described in Example 82b except starting with 1-(9,10-dihydro-9,10-methanoanthracen-9-ylcarbonyl)piperidin-4-ol (described in Example 83b), the title compound was formed in 88% yield as a white solid TLC analysis (Rf 0.59, 10% methanol in chloroform). MS (CI, CH4) m/z 306 (M+1,100), 334 (M+29,14), 288 (62), 114(8)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05455246 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-c9e6e629b82d4b94ad1d7c24d49b09d0 |
| Source note | uspto-grants-1995_10 |