HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon tetrabromide → HCID 178485422, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon tetrabromide | HCID 11205 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 178485425 | HCID 178485425 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178485422 | HCID 178485422 | 29.9% |
Reaction Steps
710 mg of trans-N-(4-chlorobenzoyl)-N-methyl-4-(4-hydroxymethylphenyl)cyclohexylamine are reacted in 20 ml of methylene chloride with 723 mg of tetrabromomethane and 572 mg of triphenylphosphine. 250 mg of the title compound are obtained, melting point 181°-183° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05455273 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-0a33907267584ec5938b90e44ab38b96 |
| Source note | uspto-grants-1995_10 |