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HRID2209802

反应详情

EQUATION

反应方程式

HRID 2209802 的结构方程式

REACTANTS

反应物

3
结构：BrC(Br)(Br)Br
HCID11205

Carbon tetrabromide

CBr4

结构：c1ccc(P(c2ccccc2)c2ccccc2)cc1
HCID11776

Triphenylphosphine

C18H15P

结构：CN(C(=O)c1ccc(Cl)cc1)[C@H]1CC[C@H](c2ccc(CO)cc2)CC1
HCID178485425

未命名化合物

PRODUCTS

生成物

1
结构：CN(C(=O)c1ccc(Cl)cc1)[C@H]1CC[C@H](c2ccc(CBr)cc2)CC1
HCID178485422

未命名化合物

收率 29.9%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

710 mg of trans-N-(4-chlorobenzoyl)-N-methyl-4-(4-hydroxymethylphenyl)cyclohexylamine are reacted in 20 ml of methylene chloride with 723 mg of tetrabromomethane and 572 mg of triphenylphosphine. 250 mg of the title compound are obtained, melting point 181°-183° C.