HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Isopropylamino)ethanol → HCID 178457051, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Isopropylamino)ethanol | HCID 7994 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178485424 | HCID 178485424 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178457051 | HCID 178457051 | — |
Reaction Steps
380 mg (1 mMol) of trans-N-(4-chlorobenzoyl)-N-methyl-4-(4-chloromethylphenyl)cyclohexylamine are reacted with 280 mg (2 mMol) of potassium carbonate and 110 mg (1.07 mMol) of 2-isopropylaminoethanol in 3 ml of dimethylformamide as described in Example 1. 259 mg (58.5% of theory) of the title compound are obtained in the form of colourless crystals, melting point 98°-100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05455273 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-d4aaa9bb5799476e80ee3104db1d17b3 |
| Source note | uspto-grants-1995_10 |