HuagongsheHuagongshe Chemistry Print Report · For research reference only
Perfluorodecanoic acid → 1-Bromoperfluorononane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Perfluorodecanoic acid | HCID 9555 | — |
| Reactant | Bromine | HCID 24408 | — |
| Reactant | Fluorine | HCID 24524 | — |
| Product | 1-Bromoperfluorononane | HCID 2776260 | 149% |
Reaction Steps
Perfluorodecanoic acid 788 g (1.53 mole), bromine 144 g (0.90 mole) and Freon 113 (200 ml) were treated with fluorine at 30°-38° C. according to the method of Example 3. Approximately 736 g of perfluorononyl bromide (88% yield) was produced. The perfluoroalkyl halide has a boiling point between 95°-6° C./20 mm Hg and a melting point of 30° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05455373 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-3350c47d622c41fca7271ddba88e0ee5 |
| Source note | uspto-grants-1995_10 |