HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2210037Generated: October 26, 2026
Benzophenone oxime → benzophenone O-{4-[5-fluoro-3-(4-methoxytetrahydropyran-4-yl)phenylthio]-alpha-methylbenzyl}-oxime
https://huagongshe.com/reaction/2210037
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzophenone oxime | HCID 11324 | — |
| Reactant | 4-{3-[4-(1-Chloroethyl)phenylthio]-5-fluorophenyl}-4-methoxytetrahydropyran | HCID 19379931 | — |
| Product | benzophenone O-{4-[5-fluoro-3-(4-methoxytetrahydropyran-4-yl)phenylthio]-alpha-methylbenzyl}-oxime | HCID 19379943 | 38% |
Reaction Steps
Using an analogous procedure to that described in Example 1 except that the reactants were heated to 60° C. for 2 hours, benzophenone oxime was reacted with 4-{3-[4-(1-chloroethyl)phenylthio]-5-fluorophenyl}-4-methoxytetrahydropyran to give benzophenone O-{4-[5-fluoro-3-(4-methoxytetrahydropyran-4-yl)phenylthio]-α-methylbenzyl}-oxime as an oil in 38% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05457125 |
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| Source dataset | uspto-grants-1995_10 |
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| ORD ID | ord-6cdcd306af894bc9ae290ec37485ca50 |
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| Source note | uspto-grants-1995_10 |
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