HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-3-pyridinesulphonamide → HCID 10727418, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-3-pyridinesulphonamide | HCID 118426 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Solvent | Propylamine | HCID 7852 | — |
| Product | HCID 10727418 | HCID 10727418 | — |
Reaction Steps
2 g of 4-chloropyridine-3-sulfonamide are dissolved in 10 cm3 of n-propylamine and 10 cm3 of isopropanol. The mixture is brought to reflux for 2 hours, the solution is then cooled and the solvent is evaporated. The solid obtained is redispersed in water (20 cm3). The insoluble material is collected on the filter, washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05459138 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-d43689a321844f498db0a0431ccd5cff |
| Source note | uspto-grants-1995_10 |