HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2210446Generated: October 31, 2026
4-Amino-3-pyridinesulfonamide → HCID 19378736, compound
https://huagongshe.com/reaction/2210446
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Amino-3-pyridinesulfonamide | HCID 10975966 | — |
| Solvent | Butyric anhydride | HCID 7798 | — |
| Product | HCID 19378736 | HCID 19378736 | — |
Reaction Steps
A mixture of 1 g of 4-aminopyridine-3-sulfonamide (Preparation 2) and 10 cm3 of butyric anhydride is heated to 180° C. for 18 hours. After cooling, the crystals obtained are collected on a filter, washed with a small amount of butyric anhydride and with diethyl ether and then dried. The product is recrystallized from hot water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05459138 |
|---|
| Source dataset | uspto-grants-1995_10 |
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| ORD ID | ord-ab5a45239e944353a2a59d3ef0c2f8a2 |
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| Source note | uspto-grants-1995_10 |
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