HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → 173158-11-7
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | Acetylbenzenesulfonyl fluoride | HCID 12821 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 173158-11-7 | HCID 962213 | — |
Reaction Steps
A solution of 20.02 g (0.1 mol) of 3-acetylbenzenesulfonyl fluoride and 29 ml of morpholine in 100 mL of THF is stirred at room temperature for 16 hours. The solvent is removed, the residue dissolved in CH2C2, and solution washed with H20 and 2N HCl. The organic layer is dried (MgSO4), the solvent removed, and the residue crystallized from CH2Cl2 -hexane to give 25.2 g (93%) of light yellow crystals, m.p. 144°-147° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05459131 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-c2644188701d44138328be6033010647 |
| Source note | uspto-grants-1995_10 |