Aluminium lithium hydride → HCID 15295460, compound

Participants

Reaction Steps

Following the procedure of Nacci et al, Vide Supra, reaction of 4(3-cyclopentyloxy-4-methoxyphenyl)-2,6-piperidinedione (12 mmol, 3.65 g) and lithium aluminum hydride (120 mmol, 4.56 g) in dry THF (240 mL) afforded the title compound as a light yellow waxy solid (2.71 g, 82%) of sufficient purity for subsequent transformations.

Provenance & Evidence