HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 15293909, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 19379004 | HCID 19379004 | — |
| Reactant | HCID 178440145 | HCID 178440145 | — |
| Product | HCID 15293909 | HCID 15293909 | 70.2% |
Reaction Steps
Following a procedure similar to that described in Example 10(a), but using 170 mg of 4-(1-hydroxy-2,2-dimethylpropyl)-2-propylimidazole-5-carbonitrile, 307 mg of methyl (4'-bromomethylbiphenyl-2-yl)glyoxylate (prepared as described in Preparation 8) and 106 mg of potassium carbonate, 257 mg of the title compound were obtained as crystals, melting at 128°-130° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05459148 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-b86d0a6a041a4bc3837b8bf7eff8f636 |
| Source note | uspto-grants-1995_10 |