HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium hydroxide, monohydrate → HCID 19378987, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium hydroxide, monohydrate | HCID 168937 | — |
| Reactant | HCID 19378945 | HCID 19378945 | — |
| Product | HCID 19378987 | HCID 19378987 | 67.8% |
Reaction Steps
680 mg of ethyl 2-ethoxymethyl-4-(1-hydroxy-1-methylethyl)-1-[(2'-methoxalylbiphenyl-4-yl)methyl]imidazole-5-carboxylate [prepared as described in step (a) above] were subjected to hydrolysis using 224 mg of lithium hydroxide monohydrate in the same manner as described in Example 1(b), to give 423 mg of the title compound as a powder, melting at 138°-140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05459148 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-6f109e0a7b89405b88c1ecdaa3209a2d |
| Source note | uspto-grants-1995_10 |