HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium hydroxide, monohydrate → HCID 19378954, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium hydroxide, monohydrate | HCID 168937 | — |
| Reactant | HCID 19378984 | HCID 19378984 | — |
| Product | HCID 19378954 | HCID 19378954 | 96.6% |
Reaction Steps
300 mg of ethyl 2-ethyl-1-[(2'-methoxalylbiphenyl-4-yl)methyl]benzimidazole-7-carboxylate [prepared as described in step (b) above] were subjected to hydrolysis using 134 mg of lithium hydroxide monohydrate in the same manner as described in Example 17(b), to give 264 mg of the title compound as a powder, melting at 278°-281° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05459148 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-f7081844fee743ecb0ebfef699236373 |
| Source note | uspto-grants-1995_10 |