HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium hydroxide, monohydrate → HCID 19378956, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium hydroxide, monohydrate | HCID 168937 | — |
| Reactant | HCID 19378998 | HCID 19378998 | — |
| Product | HCID 19378956 | HCID 19378956 | 80.8% |
Reaction Steps
252 mg of ethyl 2-ethoxy-1-[(2'-methoxalylbiphenyl4-yl)methyl]benzimidazole-7-carboxylate [prepared as described in step (a) above] were subjected to hydrolysis using 136 mg of lithium hydroxide monohydrate in the same manner as described in Example 17(b), to give 186 mg of the title compound as a powder, melting at 158°-161° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05459148 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-5d3235cb37384ff4ae5df2afced10c73 |
| Source note | uspto-grants-1995_10 |