HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Phenylethanol → HCID 19379177, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Phenylethanol | HCID 6054 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 3-(3',5'-Di-tert-butyl-4'-hydroxyphenyl)propionic acid | HCID 88389 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19379177 | HCID 19379177 | — |
Reaction Steps
3-(4-hydroxy-3,5-di-tert.-butylphenyl)-propionic acid-2-phenylethyl ester was prepared from 278 g (1 mol) of 3-(4-hydroxy-3,5-di-tert.-butylphenyl)-propionic acid and 122 g (1 mol) of 2-phenylethanol by azeotropic esterification in toluene with 0.5 g of 4-toluenesulfonic acid. The product was analyzed and the results of this analysis were as follows:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05459171 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-66892d50851c46f0986c4b910f3b5302 |
| Source note | uspto-grants-1995_10 |