Benzyl Alcohol → HCID 23205996, compound

HRID 2210590Notes

Reaction equation

HRID 2210590 reaction equation
[OH:1][C:2]1[C:7]([C:8]([CH3:11])([CH3:10])[CH3:9])=[CH:6][C:5]([CH2:12][CH2:13][C:14]([OH:16])=[O:15])=[CH:4][C:3]=1[C:17]([CH3:20])([CH3:19])[CH3:18].[CH2:21](O)[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1.C1(C)C=CC(S(O)(=O)=O)=CC=1>C1(C)C=CC=CC=1>[CH2:21]([O:15][C:14](=[O:16])[CH2:13][CH2:12][C:5]1[CH:4]=[C:3]([C:17]([CH3:20])([CH3:19])[CH3:18])[C:2]([OH:1])=[C:7]([C:8]([CH3:11])([CH3:10])[CH3:9])[CH:6]=1)[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1

Participants

5

Reactant 3

HCID 244Benzyl AlcoholHCID 6101p-Toluenesulfonic acidHCID 883893-(3',5'-Di-tert-butyl-4'-hydroxyphenyl)propionic acid

Product 1

HCID 23205996HCID 23205996, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

3-(4-hydroxy-3,5-di-tert.-butylphenyl)-propionic acid benzyl ester was prepared from 278 g (1 mol) of 3-(4-hydroxy-3,5-di-tert.-butylphenyl)-propionic acid and 108 g (1 mol) benzyl alcohol by azeotropic esterification in toluene with 0.5 g of 4-toluenesulfonic acid. The product was analyzed and the results of this analysis were as follows:

Workup

  1. customthe results of this analysis

Sources & evidence

ORD record
ord-c9f0742152b14b0caad586c4f55e5e6e
Source dataset
uspto-grants-1995_10
Patent number
US05459171

Reaction notes

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