HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 15278662, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 67805665 | HCID 67805665 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 15278662 | HCID 15278662 | 79.2% |
Reaction Steps
To a mixture of ethyl acetate (50 ml) and aqueous potassium carbonate (20 ml), 3-(3-trifluoromethyl-4-fluorophenyl)-5-methyl-2-iminothiazoline hydrochloride (1 g) was added; and the mixture was stirred. The organic layer was isolated and dried over anhydrous magnesium sulfate. The solvent was removed under reduced pressure to give 0.7 g of 3-(3-trifluoromethyl-4-fluorophenyl)-5-methyl-2-iminothiazoline as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05459277 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-58c49572741c4ae284c3cc69f2a1e5df |
| Source note | uspto-grants-1995_10 |