Methyl iodide → HCID 86749047, compound

Participants

Reaction Steps

The title compound was prepared from the N-methyl amine (0.24 g, Example 10) with methyl iodide (0.178 ml) in diethyl ether (3 ml). After 62 h the white solid which formed was isolated by filtration and washed with ether, m.p.=204°-205° C. Found: C, 46.74; H, 4.29; N, 2.41. Calcd for C22H24NOF6I.0.3H2O; C, 46.79; H, 4.39; N, 2.48%.

Provenance & Evidence