HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium hydroxide, monohydrate → HCID 19377382, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium hydroxide, monohydrate | HCID 168937 | — |
| Reactant | HCID 19377387 | HCID 19377387 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19377382 | HCID 19377382 | — |
Reaction Steps
To 0.88 g of 2-(1-acetoxy-2-fluoroethyl)-N-[(4,6-dimethoxypyrimidin-2-yl)aminocarbonyl]-3-pyridinesulfonamide in 20 ml of methanol is added 0.25 g of lithium hydroxide monohydrate. The mixture is heated to reflux for 1 hour, then allowed to cool and the methanol is evaporated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05461026 |
| Source dataset | uspto-grants-1995_10 |
| ORD ID | ord-723d3feebb0349b1a270723f5c2f249d |
| Source note | uspto-grants-1995_10 |