HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2210752Generated: October 29, 2026
HCID 19377381, compound → HCID 19377409, compound
https://huagongshe.com/reaction/2210752
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 19377381 | HCID 19377381 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 19377409 | HCID 19377409 | 100.1% |
Reaction Steps
3.6 g of 3-(1-acetoxy-2-chloroethyl)-N-(1,1-dimethylethyl)-2-pyridinesulfonamide is added to 20 ml of trifluoroacetic acid and allowed to stir at 40° C. for 12 hours. The acid is evaporated and the crude product is purified by column chromatography to give the subject compound (3 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05461026 |
|---|
| Source dataset | uspto-grants-1995_10 |
|---|
| ORD ID | ord-50fe62ba3d2e421b992dfdc1d3af9020 |
|---|
| Source note | uspto-grants-1995_10 |
|---|
