HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methoxy-1-benzothiophene → 5-Bromo-2-chloro-1-(5-methoxybenzo[b]thiophen-2-ylmethyl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methoxy-1-benzothiophene | HCID 3632425 | — |
| Reactant | 5-Bromo-2-chlorobenzaldehyde | HCID 10608925 | — |
| Product | 5-Bromo-2-chloro-1-(5-methoxybenzo[b]thiophen-2-ylmethyl)benzene | HCID 66607598 | — |
Reaction Steps
5-Methoxybenzo[b]thiophene (see WO 97/25033) and 5-bromo-2-chlorobenzaldehyde obtained in Reference Example 16-(1) were treated in a manner similar to Reference Example 9 to give the target compound. APCI-Mass m/Z 367/369 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08202984B2 |
| Source dataset | uspto-grants-2012_06 |
| ORD ID | ord-0e4678f55c5145ea9411cc571e4accd4 |
| Source note | uspto-grants-2012_06 |