反应详情

To 100 ml of concentrated hydrochloric acid, 17.2 g (62 mmole) of 1-(methoxymethyl)-6-phenylthiothymine was added and allowed to react for 2 hours at 80° C. The reaction mixture was concentrated under reduced pressure and crystallized from ethanol to obtain 3.8 g of the target compound (Yield: 26%).

1. customto react for 2 hours at 80° C
2. concentrationThe reaction mixture was concentrated under reduced pressure
3. customcrystallized from ethanol