Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | HCID 19375603 | HCID 19375603 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 14884788 | HCID 14884788 | 4.3% |
Reaction Steps
300 mg of 1-chloro-4-(2-furyl)phthalazine and 707 mg of imidazol were dissolved in 2 ml of N-methylpyrrolidone, and the solution was stirred at 150° C. for 10 hours. After the solution was subjected to after-treatment, it was purified by column chromatography, thereby obtaining 14.5 mg of 1-(1-imidazolyl)-4-(2-furyl)phthalazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05462941 |
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| Source dataset | uspto-grants-1995_10 |
|---|
| ORD ID | ord-31779b57783d4558b1f79e6f59f5ea39 |
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| Source note | uspto-grants-1995_10 |
|---|
