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HRID2211165

反应详情

EQUATION

反应方程式

HRID 2211165 的结构方程式

REACTANTS

反应物

2
结构：Br
HCID260

Hydrogen Bromide

BrH

结构：COc1ccc2cc(CCN3CC=C(c4cccc(C(F)(F)F)c4)CC3)ccc2c1.Cl
HCID19962086

未命名化合物

PRODUCTS

生成物

1
结构：Br.Oc1ccc2cc(CCN3CC=C(c4cccc(C(F)(F)F)c4)CC3)ccc2c1
HCID19962090

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

A mixture of 1-[4-(3-trifluoromethylphenyl)-1,2,3,6-tetrahydropyrid-1-yl]-2-(6-methoxy-naphth-2-yl)ethane hydrochloride (0.6 g, 0.0013 mol)(obtained as described in Example 3) and 33% HBr in acetic acid (20 ml) is refluxed for 4 hours.

WORKUP

后处理

  1. temperatureis refluxed for 4 hours