HRID2211296
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
CONDITIONS
反应条件
- 温度
- 90 °C
PROCEDURE
实验过程
Thirty five (35.0) pounds of water were added to a 22 liter vessel and heated to 90° C. Glycine (4.337 lbs.) was then added with stirring, and the solution was heated to 95° C. Zinc oxide (1.766 lbs.) was then added with stirring and heating continued for two hours until the solution was clear (gly/Zn=2.7/1; PG/Zn=3.0/1). Propylene glycol (4.94 lbs.) was then added and heating continued for an additional one-half hour.
WORKUP
后处理
- temperaturethe solution was heated to 95° C
- stirringwith stirring
- temperatureheating
- temperatureheating
- waitcontinued for an additional one-half hour