HRID2211296

反应详情

EQUATION

反应方程式

HRID 2211296 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
90 °C

PROCEDURE

实验过程

Thirty five (35.0) pounds of water were added to a 22 liter vessel and heated to 90° C. Glycine (4.337 lbs.) was then added with stirring, and the solution was heated to 95° C. Zinc oxide (1.766 lbs.) was then added with stirring and heating continued for two hours until the solution was clear (gly/Zn=2.7/1; PG/Zn=3.0/1). Propylene glycol (4.94 lbs.) was then added and heating continued for an additional one-half hour.

WORKUP

后处理

  1. temperaturethe solution was heated to 95° C
  2. stirringwith stirring
  3. temperatureheating
  4. temperatureheating
  5. waitcontinued for an additional one-half hour